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Roles of microstructures on deformation response of 316 stainless steel made by 3D printing

机译:微观结构对316 3D 3D不锈钢变形响应的作用

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One of the main challenges in additive manufacturing (AM) of metals is to manufacture high quality materials and ensure the performance of AM materials in service duties. This challenge can only be solved when the relationships between build process parameters, microstructure and deformation behaviour are understood. This present study is part of holistic efforts at Imperial College to reveal such relationships. In this study, we present our study of porosity condition, grain morphology, texture and metastable phases in AM stainless steel 316. To provide samples for mechanical and microstructural study, cylindrical samples of stainless steel 316 were printed by powder-bed laser melting with a bi-directional hatch pattern. Scanning electron microscopy and electron backscattered diffraction were used to investigate fine microstructures (such as grain morphology, texture and crystal phases) after 3D printing and deformation. Subsequently, a detailed 3D structure of columnar grains in as-printed 316 steel is constructed thanks to microscopic observation. Most of grains in as-built samples have a spherical bowl morphology, and being stacked on others to form the columnar structure. Examinations on microstructures show that the small sub-grains in as-printed samples is likely responsible for high yield strength at room temperature (significantly higher than that of conventional steel). In addition, residual stresses after rapid cooling probably promote the deformation-induced twinning that assists the plasticity during deformation, leading to a good ductility of the AM steel (almost as same as that of conventional 316 steel). Currently, a more detailed study is being undertaken to confirm this hypothesis.
机译:添加剂制造业(AM)的金属中的主要挑战之一是制造高质量的材料,并确保AM材料在服务职责中的性能。当建立过程参数,微观结构和变形行为之间的关系被理解时,才能解决这一挑战。本研究是帝国学院揭示这种关系的整体努力的一部分。在这项研究中,我们介绍了AM不锈钢316中的孔隙率,晶粒形态,质地和亚稳阶段的研究。为提供机械和微观结构的样品,通过粉床激光熔化印刷不锈钢316的圆柱形样品双向孵化图案。扫描电子显微镜和电子背散射衍射用于研究3D印刷和变形后的细微结构(如晶粒形态,纹理和晶相)。随后,由于微观观察,构建了印刷316钢中的柱状晶粒的详细3D结构。由嵌造样品中的大部分谷物具有球形碗形态,并堆叠在其他方面以形成柱状结构。关于微观结构的检查表明,印刷样品中的小亚颗粒可能在室温下高屈服强度(显着高于传统钢)。此外,快速冷却后的残余应力可能促进诱导的孪生,其有助于变形过程中的可塑性,导致AM钢的良好延展性(与传统的316钢的钢几乎一样。目前,正在进行更详细的研究以确认这一假设。

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