Optimization of process condition of nanosilica production by hydrothermal method

摘要

Bagasse ashes have high silica content thus it can be used in nanosilicaproduction to increase its benefit value. This study aimed to get the best time for synthesis and to determine the optimum synthesis time and temperature. This study used the hydrothermal method, a simple method with relatively low reaction temperature and provide a good chemical homogeneity. Time varieties in synthesizing silica were 8,10 and 12 hours, at the temperature of 150 °C. But the results were not as expected. Moreover, optimization of synthesis temperature and time used 4 hours at the temperature of 150 °C based on previous studies. Optimization was conducted using the Response Surface Methodology (RSM). Later, a testusing PSA (Particle Size Analyzer) was performed to obtain particle sizes and PDI values (Polydispersity Index). The results showed that the prediction model of temperature synthesis was 152.67 °C, synthesis time of 6 hours, particle size of 276.288 nm and PDI value of 0.189642. The tests showed that the size of particle obtained was 330.39 nm and PDI value at 0.3580. Actual results and predicted results were not significant different.