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Development of Activated Carbon from Banana Pseudo-stem via Single Step of Chemical Activation

机译:通过单一的化学激活,从香蕉伪阀开发活性炭

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Activated carbon with high surface area was successfully produced from banana pseudo-stem through a single step chemical activation process. The effect of activation parameters such as types of activating chemical (ZnCl_2 andH_3PO_4), impregnation ratios (1:1, 1:2, 1:3, 1:4 and 1:5 precursor/activating agent), activation time (30, 60, 90 and 120 min) and activation temperature (400, 500, 600, 700 and 800 °C) were evaluated based on optimum product yield and iodine number. The optimized parameters were found at impregnation ratio of 1:2 using ZnCl_2, activation time and the activation temperature of 60 min and 600 °C respectively. The product obtained from optimum parameters was further investigate using chemical and textural characteristic by using N_2 adsorption-desorption measurement, elemental analyser CHNS, SEM, FTIR. The result suggested that the AC possessed of mesoporous structure. BET surface area, total pore volume and pore diameters of the AC prepared from optimum condition were 1329.5 m~2/g, 1.16 cm~3/g and 3.8 nm respectively.
机译:通过单步化学活化过程从香蕉假阀成功生产具有高表面积的活性炭。活化参数如活化化学品(ZnCl_2和H_3PO_4),浸渍比(1:1,1:2,1:3,1:4和1:5前体/活化剂),激活时间(30,60基于最佳产物产量和碘数,评估90和120分钟)和活化温度(400,500,600,700和800℃)。使用ZnCl_2,活化时间和60分钟和600℃的浸渍比以1:2的浸渍比以优化的参数。通过使用N_2吸附 - 解吸测量,元素分析仪CHN,SEM,FTIR,进一步使用化学和纹理特性进一步研究了从最佳参数获得的产物。结果表明,AC具有介孔结构。 BET表面积,由最佳条件制备的AC的总孔体积和孔径分别为1329.5m〜2 / g,1.16cm〜3 / g和3.8nm。

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