Superfine alumina has various excellent performance, superfine aluminum often used in metallurgy, aerospace, microelectronics and medicine, so the study of alumina has become a hot research at home and abroad, superfine alumina powder the body needs are also increasing. In this paper, superfine alumina powder were prepared by hydrothermal method, and to study the preparation process. The results show that the fibrous alumina particles gradually becomes granular with the increase of pH of the reaction, pH value of 9 to get a uniform particle size distribution and an average size of small powder particles. As the increasing calcination temperature, the alumina particles gradually grow, the homogeneous superfine particulate alumina powders is obtained under calcination temperature at 950°C. The better preferred process is that alkali molar ratio of 1:3, a concentration of 0.3mol/L, the reaction temperature at 200°C, calcination temperature of 950°C.
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