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Evaluation of Thermal Shock Resistance for Ceramic Materials by Young's Modulus

机译:杨氏模量评价陶瓷材料的热抗震性能

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When a sudden temperature difference is applied to a brittle material such as ceramics, some cracks will occur in the material and it may fracture in some case. The generated cracks as a fracture origin may cause the strength reduction, so the evaluation of thermal shock resistance is very important for ceramic materials. In the conventional evaluation of the thermal shock resistance (thermal shock fracture temperature, ΔTc), the fracture stress is measured after thermal shock test as a function of temperature difference. For this method, however, many specimens are required to estimate fracture stress by bending test and the variation of the stress is large. In the present study, we tried to specify the temperature of crack initiation by measuring Young's modulus and fracture stress before and after a thermal shock test with different temperature difference. Polycrystalline alumina with high purity was used for evaluation of thermal shock resistance. The Young's modulus of all specimens was measured by resonance method, the specimen at the prescribed temperature between 200°C and 600°C, it was quickly put into water to apply thermal shock. The Young's modulus of specimens after the test was measured and the change in Young's modulus before and after thermal shock test was evaluated. Further, the specimen after the evaluation was measured the fracture strength. As a result, it was found that Young's modulus is possible to estimate thermal shock resistance. Further it is also possible to evaluate thermal shock behaviors using only one specimen.
机译:当突出的温度差施加到诸如陶瓷的脆性材料时,材料中会发生一些裂缝,并且在某种情况下可能会破裂。产生的裂缝作为裂缝起源可能导致强度降低,因此热抗冲击性的评估对于陶瓷材料非常重要。在常规评估热抗冲击性(热冲击断裂温度,ΔTc)中,在热冲击试验时测量断裂应力作为温度差的函数。然而,对于该方法,许多样本需要通过弯曲测试来估计断裂应力,并且应力的变化大。在本研究中,我们尝试通过在具有不同温度差的热冲击试验之前和之后测量杨氏模量和断裂应力来指定裂纹启动的温度。具有高纯度的多晶氧化铝用于评估热抗冲击性。所有标本的杨氏模量通过共振方法测量,在预定温度下的标本200°C和600℃,迅速投入水以施加热冲击。测量试验后的杨氏模量,评价热冲击试验前后杨氏模量的变化。此外,评估后的样品被测量裂缝强度。结果,发现杨氏模量是可以估计耐热冲击性的。此外,还可以仅使用一个样品来评估热休克行为。

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