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Two-Step Synthesis of V_2O_5 Nanosheets with High Sensing Properties toward Acetone

机译:对丙酮具有高感测性能的V_2O_5纳米片的两步合成

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Vanadium pentoxide (V_2O_5) nanosheets are successfully synthesized by a hydrothermal method, followed by a high-temperature sintering treatment. Several advanced techniques are used to characterize the morphology and composition of the nanostructures, such as transmission electron microscope (TEM), high-resolution TEM (HRTEM), scanning electron microscope (SEM), and X-ray diffraction (XRD). The HRTEM image and selected area electron diffraction (SAED) indicate the crystalline grows along [010] direction. The gas sensing performance of the V_2O_5 nanosheets was evaluated toward several volatile organic compounds (VOCs), such as ethanol, acetone, pyridine, and formaldehyde. The results show that the nanosheets exhibits superior sensing response and selectivity toward acetone to that of commercial V_2O_5 particles at optimum working temperature of ~300°C. this work will help explore vanadium oxides as sensing materials towards VOCs with high performance.
机译:五氧化二钒(V_2O_5)纳米片通过水热法成功地合成,其次是高温烧结处理。几种先进技术用于表征纳米结构的形态和组成,例如透射电子显微镜(TEM),高分辨率TEM(HRTEM),扫描电子显微镜(SEM)和X射线衍射(XRD)。 HRTEM图像和选择的区域电子衍射(SAED)表示晶体沿着方向发展。对几种挥发性有机化合物(VOC)(如乙醇,丙酮,吡啶和甲醛)评价V_2O_5纳米片的气体传感性能。结果表明,纳米片表现出优异的感测响应和对丙酮的选择性,以在〜300℃的最佳工作温度下以商业V_2O_5颗粒的选择性。这项工作将有助于探索氧化钒作为具有高性能VOC的传感材料。

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