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Preparation and Characterization of Soybean Straw Activated Carbon by Zinc Chloride

机译:氯化锌的豆秸秆活性炭的制备与表征

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The activated carbon was prepared from soybean straw by activation of zinc chloride. Porosity characterstics were determined from the analysis of N_2 adsorption isotherms using BET and BJH method. Microstructure of the sample was examined using a scanning electron microscopy. The results showed that the best sample of activated carbon was obtained under the conditions: the impregnation ratio of 3; impregnation time of 20h, activation temperature of 500°C and activation time of 90min. The iodine adsorption value, methylene blue adsorption value and phenol adsorption value were 750.67 mg/g, 168.01 mg/g and 205.36 mg/g, respectively. Activated carbon has high BET surface area (1526.54 m~2/g) and whole pore volume (0.876cm~3/g) with average pore diameter of 3.413nm.
机译:通过激活氯化锌,由大豆秸秆制备活性炭。通过使用BET和BJH法从N_2吸附等温线的分析中确定孔隙度特征。使用扫描电子显微镜检查样品的微观结构。结果表明,在条件下获得最佳活性炭样品:浸渍率为3;浸渍时间为20h,活化温度为500℃和90min的活化时间。碘吸附值,亚甲基蓝吸附值和苯酚吸附值分别为750.67mg / g,168.01mg / g和205.36mg / g。活性炭具有高BET表面积(1526.54m〜2 / g)和全孔体积(0.876cm〜3 / g),平均孔径为3.413nm。

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