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Preparation and characterization of electrospun poly(3-hydroxybutyrate-co-3-hydroxyvalerate) fibrous mats

机译:电纺聚(3-羟基丁酸酯-CO-3-羟基戊烯)纤维垫的制备与表征

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Poly (3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV), as a biodegradable polyester, was electrospun to obtain defect-free fibers with high surface-area-to-volume ratio. Several parameters such as solvent ratio, polymer concentration, applied voltage, flow rate, and tip-to-target distance were optimized to achieve defect-free morphology. The average diameter of the PHBV fibers was 1400 nm. In order to evaluate the final properties of PHBV nanofibers, the following characterization techniques were employed: scanning electron microscopy (SEM), Fourier transform infrared attenuated total reflectance (FTIR-ATR) spectroscopy, uniaxial tensile tests and dataphysics instruments.
机译:聚(3-羟基丁酸酯-CO-3-羟基戊戊烷)(PHBV)作为可生物降解的聚酯,是Electromun,以获得具有高表面积对体积比的无缺陷纤维。优化了几种参数,例如溶剂比,聚合物浓度,施加的电压,流速和尖端到靶距离,以实现无缺陷的形态。 PHBV纤维的平均直径为1400nm。为了评估PHBV纳米纤维的最终性质,采用以下表征技术:扫描电子显微镜(SEM),傅里叶变换红外衰减总反射率(FTIR-ATR)光谱,单轴拉伸试验和转息仪器。

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