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Effect of Hydroxide Concentration and Adding Ascorbic Acid on Morphology Shape of Zinc Oxide Nanostructure Prepared By Simple Chemical Precipitation Method

机译:氢氧化物浓度和添加抗坏血酸对氧化锌纳米结构形态形态的影响

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A chemical precipitation method was used to prepare zinc oxide (ZnO) nanostructure in the present of zinc nitrate and ammonium hydroxide as zinc precursor and hydroxide precursor respectively. The effect of the hydroxide concentration and the effect of adding ascorbic acid as modifier into the mixture solution on the morphology property of zinc oxide was studied. The morphology and the structural of ZnO nanostructures were investigated by field-emission scanning electron microscope (FE-SEM) and X-ray diffractometer (XRD) techniques, respectively. The results showed that the basicity solution and adding stabilizer are important parameters on the morphology and structural properties of ZnO nanostructure. At a low hydroxide concentration, ZnO exhibited flower-like structure with short petal. With a further increase to higher concentration, ZnO crystal have more crystal directional growth. When the ascorbic acid was added, the morphology changed to particle-like structure. ZnO nanostructure with different shape might be used for specific applications such as gas sensor etc.
机译:化学沉淀方法分别用于制备氧化锌(ZnO)纳米结构,分别作为锌前体和氢氧化物前体的锌氧化锌和氢氧化铵。研究了氢氧化物浓度的影响及加入抗坏血酸作为改性剂进入氧化锌氧化锌的混合物溶液中的效果。通过现场发射扫描电子显微镜(Fe-SEM)和X射线衍射仪(XRD)技术研究了ZnO纳米结构的形态和结构。结果表明,碱性溶液和添加稳定剂是ZnO纳米结构的形态和结构性质的重要参数。在低氢氧化浓度下,ZnO表现出具有短花瓣的花状结构。随着较高浓度的进一步增加,ZnO晶体具有更晶体的方向生长。加入抗坏血酸时,形态变为颗粒状结构。具有不同形状的ZnO纳米结构可用于特定应用,例如气体传感器等。

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