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Extraction and GC Determination of Volatile Aroma Compounds from Extracts of Three Plant Species of the Apiaceae Family

机译:提取和GC测定来自苹果藻家族三种植物种类萃取物的挥发性芳香化合物

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Parsley (Petroselinum crispum), dill (Anethum graveolens) and celery (Apium graveolens), three aromatic plants belonging to the Apiaceae (Umbelliferae) botanical family, were selected as sources of essential or volatile oils. Essential oils are composed of a large diversity of volatile aroma compounds. Plant-derived essential oils and extracts have long been used as natural agents in food preservation, pharmaceuticals and medicinal therapies. In the present study, the plant extracts from leaves of parsley, dill and celery, were obtained by maceration, ultrasound-assisted extraction and microwave-assisted extraction. All extractions were performed at 30°C, using different solvents (ethanol, diethyl ether, n-hexane) and solvent mixtures (1:1, v/v). The most effective solvent system for the extraction of volatile aroma compounds was diethyl ether - n-hexane (1:1, v/v). Extraction efficiency and determination of aroma volatiles were performed by GC-FID and GC-MS, respectively. The major volatile compounds present in plant extracts were myristicin, α-phellandrene, β-phellandrene, 1,3,8-p-menthatriene, apiol, dill ether and allyl phenoxyacetate.
机译:荷兰芹(Petroselinum Crispum),莳萝(Anethum Graveolens)和芹菜(Apium Graveolens),属于苹果藻(Umbelliferae)植物族的三种芳香植物,被选为必需或挥发性油源。精油由大的挥发性香气化合物组成。植物衍生的精油和提取物长期以来已被用作食品保存,药物和药物疗法的天然剂。在本研究中,通过浸渍,超声波辅助提取和微波辅助提取获得来自欧芹,莳萝和芹菜叶的植物提取物。所有萃取均在30℃下进行,使用不同的溶剂(乙醇,乙醚,正己烷)和溶剂混合物(1:1,v / v)。用于提取挥发性香气化合物的最有效的溶剂系统是乙醚 - 正己烷(1:1,V / V)。通过GC-FID和GC-MS分别进行提取效率和香气挥发物的测定。植物提取物中存在的主要挥发性化合物是肉豆蔻蛋白,α-磷锡,β-磷锡,1,3,8-p-inhathaterne,Apiol,荷醚和烯丙基苯甲酸酯。

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