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Study of Photocatalytic activity and properties of Transition metal ions doped Nanocrystalline TiO2 prepared by Sol-Gel Method.

机译:溶胶 - 凝胶法制备的光催化活性及过渡金属离子掺杂纳米晶体TiO2的性能研究。

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We report the growth of [Fe, Co]_xTiO2 (x=0.01,0.02 &0.04) nanocrystals prepared by Sol-Gel techniqu, followed by freeze-drying treatment at -30°C temperature for 12hrs. The obtained Gel was thermally treated at different temperature like 200,400,600, 800°C. We studied its Structural, Photocatalytic and magnetic properties by using X-ray diffraction, Scanning Electron microscopy (SEM), Energy dispersive X-ray spectroscopy (EDAX) and Gouy Balance techniqu. The as-prepared samples are found to be paramagnetic at room temperature. The photoreactivity of transition metal ion-doped TiO2 nanoparticles under UV irradiation were quantified by the degradation of formaldehyde.
机译:我们报告了通过溶胶 - 凝胶技术制备的[Fe,Co] _XxiO2(X = 0.01,0.02&0.04)纳米晶体的生长,然后在-30℃温度下冷冻干燥处理12小时。将所得凝胶在不同温度下热处理,如200,400,600,800℃。我们通过使用X射线衍射,扫描电子显微镜(SEM),能量分散X射线光谱(EDAX)和粪便平衡技术来研究其结构,光催化和磁性。发现如制备的样品在室温下是顺磁性。通过甲醛的降解量化过滤金属离子掺杂TiO2纳米颗粒的光反应性通过甲醛的降解量化。

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