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Influence of Sargassum crassifolium Extract on the Absorption of Magnetic Iron Oxide Nanoparticle via Green Synthesis Route

机译:Sargassum Crassifolium提取物对绿色合成途径磁性氧化铁纳米粒子吸收的影响

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This work reported the influence of seaweed (Sargassum crassifolium) extract on the absorption of magnetic iron oxide nanoparticles (MIONPs) via green synthesis route. The seaweed extract acted as reducing and capping agent. Ultraviolet-visible (UV-Vis) spectra revealed the presence of sharp peaks at around 366 nm to 371 nm which corresponds to the absorption spectra of MIONPs. The absorption peaks corresponding to MIONPs was significantly affected by the varying amount of seaweed extract. On the other hand, Fourier Transform- Infrared (FTIR) spectra revealed the presence of the vibration mode around 532 cm~(-1) to 551 cm~(-1) which corresponds to Fe-O bands suggesting the successful formation of MIONPs. Thermogravimetric (TGA) spectra showed that the produced MIONPs stabilizes at 400 °C. The synthesized MIONPs are spherical in shape with an estimated average diameter of 20 nm as revealed by the Field Emission Scanning Electron Microscopy (FESEM). Finally, the produced MIONPs exhibit magnetic property via attraction with an external magnet. This straight forward green synthesis of MIONPs can be a good route for possible industrial and environmental application.
机译:这项工作报告了海藻(Sargassum Crassifolium)提取物对通过绿色合成途径对磁性氧化铁纳米颗粒(MIONPS)的吸收的影响。海藻提取物充当了还原和封盖剂。紫外 - 可见(UV-VI)光谱显示出锐峰的存在,约为366nm至371nm,其对应于MiOnps的吸收光谱。对应于MIONPS的吸收峰受到不同量的海藻提取物的显着影响。另一方面,傅里叶变换 - 红外线(FTIR)光谱显示出振动模式的存在约532cm〜(-1)至551cm〜(-1),其对应于表明术语成功形成的FE-O频段。热重量(TGA)光谱表明,所生产的肿瘤在400℃下稳定。合成的MIONPS呈形状的球形,估计平均直径为20nm,如现场发射扫描电子显微镜(FESEM)所揭示的。最后,所产生的MIONPS通过用外部磁铁的吸引力表现出磁性。这种直线绿色合成的MiONPS可以是可能的工业和环境应用的好路线。

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