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Facile synthesis of SnS microrods films prepared by electrochemical Deposition

机译:通过电化学沉积制备的SNS微孔膜的体积合成

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Despite plenty of reports on the preparation of SnS films, it remains challenging to grow SnS microrods films. In this paper, we describe a facile synthesis of the SnS microrods films, utilizing constant potential cathodic electro-deposition method, as well as the investigation of its structure and optical properties. The synthesis involves a mixture of stannous sulfate, EDTA and sodium thiosulfat. Preliminary studies on the growth mechanism indicate that SnS films are preferentially oriented along the (101) plane, which is quite different from the previous report that oriented along the (111) plane. Raman spectra indicate that the microrods films have a high purity.
机译:尽管有大量的报道编写SNS薄膜,但仍然持挑战性剧本。在本文中,我们描述了SNS微孔膜的容易合成,利用恒定的潜在阴极电沉积方法,以及其结构和光学性能的研究。合成涉及亚硝酸亚锡,EDTA和硫代硫酸钠的混合物。对生长机理的初步研究表明,SNS膜优先沿(101)平面取向,这与沿(111)平面定向的先前报告完全不同。拉曼光谱表明Microrod薄膜具有高纯度。

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