Preparation, Spectral Characterization and Crystal Structure 2-Acetyl-2'-methoxyIacetaniIide

摘要

2-Acetyl-2'-methoxylacetanilide has been synthesized by the reaction of 2-methoxylaniline and ethyl acetoacetate in toluene solution. The compound was characterized by MS, Infrared spectrum, ~1HNMR and X-ray single crystal diffraction analysis. The results show that the compound is target product. The crystal data for 2-acetyl-2'-methoxylacetanilide: monoclinic, space group P2(l)/c, Mr= 207.22, De = 1.309 g/cm~3, F (000) = 440, R = 0.0826 and wR = 0.1822. The complex forms layered structure through ?---? stacking interaction.