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Preparation of Polyurethane (PU)/Polyaniline (PANI) compound nanofiber via electrospinning

机译:通过静电纺丝制备聚氨酯(PU)/聚苯胺(PANI)化合物纳米纤维

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In this paper polyurethane (PU)/polyaniline (PANI) nanofibers were successfully prepared via electrospinning with N, N-dimethylformamide (DMF) and tetrahydrofuran (THF) mixture (1:2 mass ratio). The morphology, diameter and structure of the electrospun nanofibers were examined by scanning electron microscopy (SEM) and the diameter distribution of nanofibers was measured by Image-Pro Plus. Results indicate that the morphology, diameter and uniformity of the fibers were influenced by solution concentration, applied voltage, capillary-screen distance and flow rate greatly, and the finer and uniform nanofibers were electrospun from total solid content of the spinning solutions at 8 wt.%, PU and PANI with ratio of 10/1 (w/w), the spinning voltage at 35 kV, the collecting distance at 15 cm and the extruding speed at 6 ml/h.
机译:在本文中,通过用N,N-二甲基甲酰胺(DMF)和四氢呋喃(THF)混合物(1:2质量比)来成功制备聚氨酯(PU)/聚苯胺(PANI)纳米纤维。通过扫描电子显微镜(SEM)检查电纺纳米纤维的形态,直径和结构,通过图像Pro加上纳米纤维的直径分布。结果表明,纤维的形态,直径和均匀性受到溶液浓度,施加的电压,毛细管 - 距离和流速的影响,并且较好且均匀的纳米纤维在8wt时从纺丝溶液的总固体含量进行电纺。 %,PU和PANI以10/1(w / w),纺丝电压为35kV,收集距离为15cm,挤出速度为6ml / h。

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