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Preparation and Property of Hydrophobic Modified Guar Gum Thickener

机译:疏水性改性瓜尔胶增稠剂的制备及性能

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The modified guar gum was synthesized with guar gum as material and bromododecane as etherifying agent by suspension polymerization method. The solution and gel of the modified guar gum were also prepared. The structure and the property of the modified guar gum were analysized by Fourier transform infrared spectrum (FT-IR), X-ray diffraction (XRD) and thermogravimetric analysis (TGA). The heat resistance and the viscoelasticity modulus of the gel were also researched by rheometer. The results of FT-IR and XRD show that the hydrophobic long chain has been introduced into the guar gum successfully. TGA indicates that the modified guar gum has higher thermal stability. The rheology tests reflect that with different temperature conditions, the shear viscosity, the viscoelasticity modulus of the gel and the heat resistance of the modified guar gum are both better than that of the unmodified guar gum. The modified guar gum can be used as thickener of fracturing fluid, and it can reduce its amount.
机译:通过悬浮聚合方法用瓜尔胶作为材料和溴二癸烷合成改性的瓜尔胶作为醚化剂合成。还制备了改性瓜尔胶的溶液和凝胶。通过傅里叶变换红外光谱(FT-IR),X射线衍射(XRD)和热重分析(TGA)分析改性瓜尔胶的结构和性质。通过流变仪研究凝胶的耐热性和粘弹性模量。 FT-IR和XRD的结果表明,疏水性长链已成功引入瓜尔胶中。 TGA表示改良的瓜尔胶具有较高的热稳定性。流变术试验反映,在不同的温度条件下,凝胶粘度,凝胶的粘弹性模量和改性瓜尔胶的耐热性均比未改性的瓜尔胶胶。改性瓜尔胶可以用作压裂液的增稠剂,可以减少其量。

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