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Study on Preparation and Tribology Behaviors of Ni-P Electroless Deposited Nanocrystalline Coating

机译:Ni-P化学沉积纳米晶体涂层的制备及摩擦学行为研究

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Ni-P nanocrystalline and amorphous coating were fabricated by electroless deposition technique in the same bath except for varying complexing agent. Heat treatment at lower temperature was carried out to the two kinds of coatings above. The phosphorus content and organize structure of the as-deposited coatings was determined by means of inductively coupled plasma atomic emission spectrometry, X-ray diffractometer and transmission electron microscope. Moreover the effects of heat treatment and structure on microhardness and tribology property of coatings were studied by means of microhardness tester, friction and wear tester and scanning electron microscope. Outstanding tribology property of Ni-P nanocrystalline coating compared with the amorphous one owed to the fine nickel grains with a size of several nanometers. While the proper heat treatment process was found to be responsible for improved property of both coatings.
机译:除了不同络合剂外,通过在相同浴中的无电沉积技术制造Ni-P纳米晶和无定形涂层。在上面的两种涂层中进行较低温度的热处理。通过电感耦合等离子体原子发射光谱法,X射线衍射仪和透射电子显微镜测定磷酸含量和组织结构。此外,通过微硬度测试仪,摩擦和磨损测试仪和扫描电子显微镜研究了热处理和结构对微硬度和摩擦学性质的影响。与尺寸为几纳米尺寸的优异镍晶粒相比,Ni-P纳米晶体涂层的突出杂散性。虽然发现适当的热处理过程负责两种涂层的改善性质。

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