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The Influence Research of Cu~(2+) on Cu_xFe_(1-x)O.Fe_2O_3 Magnetic Fluids

机译:Cu〜(2+)对Cu_XFE_(1-X)O.FE_2O_3磁流体的影响研究

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In order to increase the magnetic fluids in target-based cancer treatment, the Cu~(2+) has been studied in this study. The Fe_3O_4 and Cu_(0.1)Fe_(0.90)Fe_2O_3 magnetic nanoparticles were prepared by ultrasonic emulsion method, and then disperse them into water with sodium dodecyl benzene sulfonate (SDBS) as surfactants to make magnetic fluids. The cubic inverse spinel structure of Fe_3O_4 and Cu_(0.1)Fe_(0.90)Fe_2O_3 nanoparticles were analyzed by X-ray diffraction technique (XRD).The saturation magnetization of Fe_3O_4 and Cu_(0.1)Fe_(0.90)Fe_2O_3 were 79.55 emu.g~(-1) and 75.90 emu.g~(-1) by vibrating sample magnetometer (VSM). The morphologies of nanoparticles were observed by transmission electron microscope (TEM). The particle size was uniform 10-20 nm, and their shape was approximately spherical. The Cu_(0.1)Fe_(0.9)O.Fe_2O_3 magnetic particle functional group and the surface of particle coated with SDBS have been detected by Fourier Transform Infrared Spectroscopy (FT-IR). The magnetic fluids with a high saturation magnetization and stability have been prepared successfully in this study.
机译:为了增加基于目标的癌症治疗中的磁性流体,本研究已经研究了Cu〜(2+)。通过超声波乳液法制备Fe_3O_4和Cu_(0.1)Fe_(0.90)Fe_2O_3磁性纳米颗粒,然后用十二烷基苯磺酸钠(SDB)作为表面活性剂将它们分散到水中以制造磁性流体。通过X射线衍射技术(XRD)分析Fe_3O_4和Cu_(0.1)Fe_(0.90)Fe_2O_3纳米颗粒的立方反向尖晶石结构。Fe_3O_4和Cu_(0.1)Fe_(0.90)Fe_2O_3的饱和磁化为79.55 emu.g通过振动样品磁力计(VSM)〜(-1)和75.90 emu.g〜(-1)。通过透射电子显微镜(TEM)观察纳米颗粒的形态。粒度为10-20nm均匀,它们的形状约为球形。通过傅里叶变换红外光谱(FT-IR)检测Cu_(0.1)Fe_(0.9)O.Fe_2O_3磁性颗粒官能团和涂覆有SDB的颗粒表面。在该研究中成功地制备了具有高饱和磁化和稳定性的磁性流体。

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