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Preparation and Characterization of SnO_2/TiO_2 Composite with Low infrared Emissivity

机译:具有低红外发射率的SnO_2 / TiO_2复合材料的制备与表征

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SnO_2/TiO_2 composite material was prepared by use of microwave deposition method, on basis of tetrabutyl titanate(C_(16)H_(36)O_4Ti) and tin tetrachloride(SnCl_4) were used as source material and carbamide (CO(NH_2)_2) as precipitator. The characteristics of composite material were investigated by means of X-ray diffraction (XRD), scanning electron microscope(SEM) and Fourier transform infrared(FTIR). The result showed that optimization mol ratio of carbamide and metal elementary( Sn & Ti) was 2:1. SnO_2 adulteration counterworked TiO_2 crystal transformation and restrained rutile nucleation. Anatase TiO_2 grew up easily. SnCh content had been influence on composite material average emissivity at 8~14 ìm waveband. Mix proportion of composite material was achieved which emissivity was 0.3185.
机译:通过使用微波沉积方法制备SnO_2 / TiO_2复合材料,基于四丁酯(C_(16)H_(36)O_4TI)和四氯化锡(SNCL_4)作为源材料和氨基甲酸酯(CO(NH_2)_2)作为除尘器。通过X射线衍射(XRD),扫描电子显微镜(SEM)和傅里叶变换红外(FTIR)研究了复合材料的特性。结果表明,碳酰胺和金属基本(Sn&Ti)的优化摩尔比为2:1。 SnO_2掺假逆算TiO_2晶体转化和受限制的金红石成核。 Anatase TiO_2很容易增长。 SNCH含量在8〜14μm波段处对复合材料平均发射率的影响。实现复合材料的混合比例,发射率为0.3185。

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