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Solgel Self-combustion Synthesis and characterization of La_(0.8)Sr_(0.2)Mn_(0.8)Fe_(0.2)O_3

机译:La_(0.8)Sr_(0.2)Mn_(0.8)Fe_(0.2)O_3的La_(0.8)SRG的粘接性合成和表征

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La_(0.8)Sr_(0.2)Mn_(0.8)Fe_(0.2)O_3 has been synthesized by solgel synthesis employing the EDTA complexing method and solgel self combustion using PVA as fuel and nitrates as oxidizing agent. The effect of these techniques on the phase purity, crystallinity and particle size has been studied. Different techniques including X-Ray Diffraction (XRD), Scanning electron microscopy (SEM), Thermo gravimetric/Differential thermal analysis (TG/DTA) and Inductively Coupled Plasma Emission Spectrometry (ICP-ES) have been utilized for the characterization of the synthesized materials.
机译:La_(0.8)Sr_(0.2)Mn_(0.8)Fe_(0.2)Fe_3已经通过溶胶合成合成,采用EDTA络合方法和使用PVA作为燃料和硝酸盐作为氧化剂的溶胶自燃烧。研究了这些技术对相纯度,结晶度和粒度的影响。已经利用了包括X射线衍射(XRD),扫描电子显微镜(SEM),热重谱/差分热分析(TG / DTA)和电感耦合等离子体发射光谱法(ICP-ES)的不同技术已经用于合成材料的表征。

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