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Coarsening during Sintering

机译:在烧结期间粗化

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摘要

Early treatments of sintering realized that grain size was an important metric for predicting the sintering rate. As well, properties of sintered materials pivot around grain size. With nanoscale powders there is a greater demand for coarsening control during sintering. The conditions needed to induce sintering depend on the material and a host of processing variables. During sintering there is significant microstructure coarsening, evident as grain growth and pore growth via interlaced events including changes in porosity, pore size, grain coordination, interface wetting, and grain boundary area. After an initial transient, sintering converges to a self-similar grain shape and grain size distribution. For sintering microstructures microstructure evidences both complexity (multiple interfaces with changing compositions and morphology) and simplicity (only a few parameters genuinely dictate coarsening). These relations are summarized here to show how grain coarsening can be treated during sintering.
机译:烧结的早期处理意识到粒度是预测烧结率的重要指标。同样,烧结材料的性质枢转围绕晶粒尺寸。纳米尺度粉末在烧结过程中对粗化控制有更大的需求。诱导烧结所需的条件取决于材料和一系列处理变量。在烧结过程中,具有显着的微观结构粗糙化,视发晶粒生长和孔生长通过隔行扫描事件,包括孔隙率,孔径,晶粒配位,界面润湿和晶界区域的变化。在初始瞬态之后,烧结收敛到自相似的晶粒形状和晶粒尺寸分布。对于烧结微观结构微观结构证明复杂性(多种接口改变组成和形态学)和简单性(只有几个参数真正指挥粗化的参数)。这些关系总结在这里,以展示在烧结期间可以治疗谷粒粗化。

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