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Effect of Carburization Process on Adhesion Strength of Ti Carbide Layer on Titanium Alloy Substrate

机译:渗碳工艺对钛合金基质Ti碳化物层粘附强度的影响

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Titanium alloys are commonly used in biomedical application in hard tissues replacement especially for knee and hip implants. Surface modifications are required prior to diamond coating process for improving tribological and wear properties of the titanium alloy. In this study, experiments were carried out to investigate the effects of different carburizing times on the adhesion strength of carbide layer formed on the Ti-6Al-7Nb. Prior to carburization process, all samples were treated to remove residual stress and oxide scales by annealing and pickling processes respectively. Hard wood charcoal powder was used as a medium. The carburizing process was carried out for 6, 12 and 24 hours at 950°C under normal atmospheric condition. Surface morphology, carbide layer thickness and adhesion strength were evaluated using SEM, XRD, 3D Surface Profilometer and Blast Wear Tester (BWT). It is found that a mixture of oxide and carbide layers formed on the substrate and the thickness of these layers increases with carburizing time. It is also revealed that the 24 hr carburizing time provides the strongest adhesion strength among the three and TiC as the dominant layer.
机译:钛合金常用于生物医学应用中的硬组织替代品,特别是对于膝关节和臀部植入物。在金刚石涂覆方法之前需要表面修饰,以改善钛合金的摩擦磨损性能。在该研究中,进行实验以研究不同渗碳时间对在Ti-6AL-7NB上形成的碳化物层的粘附强度的影响。在渗碳过程之前,处理所有样品以分别通过退火和酸洗方法去除残余应力和氧化物鳞片。使用硬木炭粉末作为培养基。在正常大气条件下在950℃下进行渗碳过程6,12和24小时。使用SEM,XRD,3D表面轮廓仪和喷涂测试仪(BWT)评估表面形态,碳化层厚度和粘合强度。发现在基板上形成的氧化物和碳化物层的混合物和这些层的厚度随渗碳时间而增加。还揭示了24小时渗碳时间为三个和TIC中的最强的粘合强度提供为显性层。

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