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Study on Preparation Technique of SiC/Cu-Al Composite by Pressureless Infiltration

机译:无气压渗透的SiC / Cu-Al复合材料制备技术研究

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In order to improve the compatibility between SiC particles and aluminum, the SiC/Cu composite powders were prepared by using chemical plating method to coat a Cu layer on the SiC particles surface. The obtained powders were made into preform and then put it into molten aluminium. SiC/Cu-Al composite were produced by using pressureless infiltration method under argon gas. By scanning electron microscopy (SEM), optical microscopy (OM), X-ray diffraction (XRD), the phase structure and microstructure of SiC/Cu composite powders and SiC/Cu-Al composite were analysed. Moreover, the temperature and soaking time on the effect of SiC/Cu-Al composite infiltration depth and effect were studied. The results show that: Cu coating on the SiC particles surface distributed uniformly; SiC/Cu-Al composite prepared at the condition of 800°C and 2 hours soaking time has a densification microstructure, SiC particles uniformly distributed in the aluminum matrix and there is no Al_4C_3 brittle phase formation; at 700°C~900°C infiltration, as the temperature growing, infiltration depth increases at first and then decreases; the microstructure of SiC/Cu-Al composite which infiltrated 2 hours is more compact than that 1 hour; Cu coating effectively improved the wettability between SiC particles and molten aluminum, and inhibited the formation of harmful interfacial reaction.
机译:为了提高SiC颗粒和铝之间的相容性,通过使用化学镀方法在SiC颗粒表面上涂覆Cu层来制备SiC / Cu复合粉末。将所得粉末制成预制件,然后将其放入熔融铝中。通过在氩气下使用无压渗透方法制备SiC / Cu-Al复合材料。通过扫描电子显微镜(SEM),分析光学显微镜(OM),X射线衍射(XRD),SiC / Cu复合粉末和SiC / Cu-Al复合材料的相结构和微观结构。此外,研究了SiC / Cu-Al复合渗透深度和效果效果的温度和浸泡时间。结果表明:SiC颗粒表面上的Cu涂层均匀分布; SiC / Cu-Al复合材料在800℃和2小时的条件下浸泡时间具有致密化微观结构,均匀分布在铝基中的SiC颗粒,没有Al_4C_3脆性相;在700°C〜900°C渗透,随着温度的增长,渗透深度首先增加,然后减少;渗透2小时的SiC / Cu-Al复合材料的微观结构比1小时更紧凑; Cu涂层有效改善了SiC颗粒和熔融铝之间的润湿性,并抑制了有害界面反应的形成。

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