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Performance of a Planar Micro-Flame Ionization Detector

机译:平面微火焰电离检测器的性能

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The flame ionization detector (FID) is the preferred method of hydrocarbon detection. Unfortunately, it is operated at high fuel and oxidant gas flow and therefore not suitable for portable applications. This work presents an FID miniaturized by means of MEMS technology (μFID) to reduce gas consumption. Before, the minimum detectable limit (MDL) of the μFID used to be a factor 20 above what can be expected from conventional FIDs. This paper presents two approaches that lead to improved device performance. First, the fuel gas flow is increased, which results in larger flames with higher ionizing power and a reduction of the MDL by a factor 1.24. Then, premixing the sample gas with the fuel gas, instead of separate sample gas supply, allows for a further reduction of the MDL by a factor 2.12.
机译:火焰电离检测器(FID)是烃检测的优选方法。不幸的是,它在高燃料和氧化剂气流下操作,因此不适合便携式应用。这项工作提出了一种通过MEMS技术(μFID)小型化的FID,以降低气体消耗。之前,μFID的最小可检测限制(MDL)用于高于传统FIDS可以预期的因素20。本文提出了两种方法,导致设备性能提高。首先,燃料气体流量增加,这导致具有更高电离功率的较大火焰和MDL的减少因子1.24。然后,用燃料气体预混合,代替单独的样品气体供应,允许进一步减少MDL的因子2.12。

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