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Morphology Characterization and Optical Properties Analysis for Nanostructured Lanthanum Hexaboride Powders

机译:纳米结构镧六硼化粉粉体的形态学特征及光学性质分析

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Nanostructured Lanthanum hexaboride (LaB_6) powders were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM) and X-ray photoelectron spectra (XPS). The average size of LaB_6 nanoparticles is about 35 nm, which are well crystallized with ball or ellipsoid with inconspicuous corners and covered by a 3-5 nm thick amorphous layer containing oxygen and carbon. The absorption of LaB_6 nanoparticles in visible and near infrared spectrum (NIR) was measured and compared with micron scale particles. The surface plasmon responance (SPR) of nanoparticles was very efficient at NIR blocking, which almost covered the whole NIR region. The influence of nanoparticles concentration on spectrum absorption was comparatively evident. Meanwhile, micron particles almost haven't NIR blocking function.
机译:通过X射线衍射(XRD),透射电子显微镜(TEM),高分辨率透射电子显微镜(HRTEM)和X射线光电子能谱(XPS)以X射线衍射(Lab_6)粉末特征在于纳米结构镧(Lab_6)粉末。 Lab_6纳米颗粒的平均尺寸约为35nm,其与球或椭圆体具有不显眼的角落,并由含有氧和碳的3-5nm厚的无定形层覆盖。测量并与微米级颗粒进行测量并与微米级颗粒进行测量并与近红外光谱(NIR)中的Lab_6纳米颗粒的吸收。纳米颗粒的表面偏移(SPR)在NIR阻塞时非常有效,几乎覆盖了整个NIR区域。纳米颗粒浓度对光谱吸收的影响相对明显。同时,微米颗粒几乎没有鼻塞阻挡功能。

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