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Synthesis Of MgO Nano-Cubes On Si (001) By Thermal Evaporation

机译:热蒸发合成Si(001)的MgO纳米立方体

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MgO nano-cubes have been successfully deposited on Si (001) substrates using a thermal evaporation method at 800°C without using a catalyst. The as-synthesized products were characterized by variable pressure scanning electron microscopy (VPSEM), X-Ray diffraction (XRD), UV-Visible spectroscopy and BET measurements. VPSEM results showed sharp-edged of three dimensional cubes of MgO, ranging from 50 nm to 300 nm in diameter. The sharp peaks in the XRD pattern indicated high crystallinity with a face centered-cubic MgO structure. The value of the optical band gap energy from the transmission spectrum was 4.86 eV, whereas the specific surface area of the MgO nano-cube was 190.1 m~2/g.
机译:在不使用催化剂的情况下在800℃下使用热蒸发方法成功地沉积在Si(001)底物上成功沉积在Si(001)底板上。通过可变压力扫描电子显微镜(VPSEM),X射线衍射(XRD),UV可见光光谱和BET测量来表征AS合成的产品。 VPSEM结果显示了MgO的三维立方体的尖锐边缘,直径为50nm至300nm。 XRD图案中的尖锐峰表示高结晶度与面部中心立方MgO结构。来自透射光谱的光带间隙能量的值为4.86eV,而MgO纳米立方体的比表面积为190.1m〜2 / g。

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