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Synthesis and Characterizations of Nanocubes, Monodispersed Nanocrystals and Nanospheres of Au

机译:纳米孔,单分散纳米晶体和Au纳米球体的合成与表征

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Nanocubes, monodispersed nanocrystals and nanospheres of Au have been prepared by a simple reaction between HAuCl_4·4H_2O, NaOH and NH_2OH·HCl in the presence of gelatin. The role of gelatin and the affection of pH in producing the nanoparticles of Au were discussed. The products were characterized by X-ray powder diffraction, transmission electron microscopy, and UV-visible absorption spectroscopy. The sizes of the monodispersed nanocrystals of Au were estimated by Debye-Scherrer formula according to XRD spectrum.
机译:在明胶存在下,通过Haucl_4·4H_2O,NaOH和NH_2OH·HCl之间的简单反应制备了纳米孔,单分散的纳米晶体和Au的纳米球。讨论了明胶的作用和pH在制备Au纳米粒子中的影响。该产品的特征在于X射线粉末衍射,透射电子显微镜和UV可见吸收光谱。根据XRD光谱,通过Debye-Scherrer公式估算Au的单分散纳米晶体的尺寸。

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