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Preparation of Nanoporous Super Thermal Insulation Material Compounded with Xonotlite-SiO{sub}2-Aerogel and Characterization of the Pore Structure

机译:用Xonotlite-SiO {Sub} 2 - 气凝胶配混的纳米多孔超热绝热材料的制备及孔隙结构的表征

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Ultra-light calcium silicate material constructed with fibrous xonotlite crystals has an advantage of low-thermal conduction coefficient. But the microporous structure can hardly make a better performance in terms of super thermal insulation. Although nanoporous structure of SiO{sub}2-aerogel satisfies the requirement, its tenacity is not strong enough to produce by itself blocky super thermal insulation material. This research, thus proposes to apply SiO{sub}2-aerogel as nanoporous carrier in the process of preparation, with Ultra-light calcium silicate material constructed with fibrous xonotlite crystals as the matrix so as to prepare nanoporous super thermal insulation material compounded with Xonotlite-SiO{sub}2-aerogel via so-gel method and ethanol supercritical drying. SEM and pore size distribution techniques were here applied to characterize the morphology and pore structure of the composite material. The results show that the SiO{sub}2-aerogels were better distributed in pore of calcium silicate matrix, with the pore size distribution of composite ranging from 10 nanometers to 50 nanometers, and average pore size less then 20 nm.
机译:用纤维Xonotlite晶体构造的超光硅酸钙材料具有低热导通系数的优点。但微孔结构在超级绝热方面几乎不能更好地进行性能。虽然二氧化硅{子} 2 - 气凝胶满足以下要求的纳米多孔结构,其韧度不够强本身以产生块状超绝热材料。本研究,从而提出申请的SiO {子} 2 - 气凝胶如在制备过程中的纳米多孔载体,具有与纤维硬硅钙石晶体为基体构成超轻硅酸钙材料以制备具有硬硅钙石复合纳米多孔超级绝热材料-SiO {子}通过这样 - 凝胶法和乙醇超临界干燥2 - 气凝胶。这里施加SEM和孔径分布技术以表征复合材料的形态和孔结构。结果表明,在SiO {子} -2-气凝胶更好分布在硅酸钙基质的孔隙,与复合材料的孔径分布范围从10纳米至50个纳米,且平均孔径小于20纳米。

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