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SINTERING OF OXIDE CERAMICS UNDER RAPID MICROWAVE HEATING

机译:快速微波加热下氧化陶瓷烧结

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Rapid microwave sintering of Y2O3 nanopowder samples has been investigated. Using a 24 GHz / 6 kW gyrotron system for microwave processing of materials, the compacted powder samples were heated at rates in the range 10...200 °C/min to maximum temperatures 1400... 1700 °C with zero hold time. At higher heating rates a sharp increase in the material's effective conductivity has been observed, which is similar to the flash sintering effect. Maximum densities of the sintered Y2O3 samples, above 98 %, have been obtained with a heating rate of 100 °C/min and maximum temperatures 1600...1700 °C. The duration of the high-temperature stage of sintering was about 8 min and the microwave power absorbed in the samples, per unit volume, was about 40 W/cm~3.
机译:研究了Y2O3纳米粉末样品的快速微波烧结。使用24 GHz / 6 kW Gyrotron系统进行材料的微波处理,将压实的粉末样品以10 ... 200°C / min的范围内加热到最大温度1400 ... 1700°C,零容量。在更高的加热速率下,已经观察到材料有效导电性的急剧增加,这类似于闪光烧结效果。已经获得了烧结的Y2O3样品的最大密度,高于98%,得到100℃/ min的加热速率和最大温度1600 ... 1700℃。烧结高温阶段的持续时间约为8分钟,每单位体积的样品中吸收的微波功率为约40W / cm〜3。

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