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Scanning Electron Microscopy and Roughness Measurements of the Wear Scars Generated in Carbide Composites by the ASTM B611 Test

机译:ASTM B611试验扫描电子显微镜和碳化物复合材料中产生的磨损疤痕的粗糙度测量

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Abrasion resistance of conventional cemented carbides such as WC-Co where the hard particles are typically a few microns in size and non-conventional carbide composites such as DC carbide composites where the hard phase is a sintered WC-Co pellet several tens of microns in size was measured using the ASTM B611 wear test. All the wear data are uniformly expressed in terms of wear coefficients, defined as volume lost per unit load and unit sliding distance. Wear coefficients of cemented WC-Co show excellent correlation to bulk hardness. Wear coefficients for DC carbide, however, deviate significantly from this trend and the values are exceptionally low for their level of hardness. Typical wear scars generated by the B611 test are asymmetric with the exit side more sharply defined than the entry side. Roughness measurements along the length of the wear scar show that the roughness varies in a systematic way from the entry to the exit side. For WC-Co cemented carbides the average and maximum roughness values at the exit end and the peak of the roughness profile show good correlation to bulk hardness. Roughness values for the DC carbides also fall on the same lines. Scanning electron microscopy and energy dispersive analysis of the wear scars show embedded and fractured alumina particles of different sizes and amounts in all of the wear scars. For DC carbides the embedded alumina particles are found preferentially in the binder areas, whereas for WC-Co cemented carbides, the alumina particles are more uniformly distributed. We suggest a mechanism for the preferential embedding of alumina particles in the binder areas of DC composites and claim that such preferential embedding is responsible for the observed low wear coefficients for these composites as compared to conventional WC-Co.
机译:常规硬质碳化物的耐磨性,如WC-Co,其中硬颗粒通常是尺寸和非常规碳化物复合材料的诸如DC碳化物复合材料的诸如DC碳化物复合材料,其中硬相是烧结WC-CO颗粒的尺寸为几十微米使用ASTM B611磨损试验测量。所有磨损数据都以磨损系数均匀地表达,定义为每单位负载和单元滑动距离损失的体积。粘合WC-Co的磨损系数显示出与散装硬度的良好相关性。然而,DC硬质合金的磨损系数显着偏离这种趋势,并且对于它们的硬度水平非常低。由B611测试产生的典型磨损疤痕与出口侧比入口侧更加尖锐地,不对称。沿磨损瘢痕的长度的粗糙度测量表明,粗糙度从进入出口侧的系统方式变化。对于WC-Co粘合的碳化碳,出口端的平均值和最大粗糙度值和粗糙度曲线的峰值显示出与散装硬度的良好相关性。 DC碳化物的粗糙度值也落在相同的线上。扫描电子显微镜和磨损疤痕的能量分散分析显示嵌入式和裂缝氧化铝颗粒的不同尺寸和所有磨损疤痕的量。对于DC碳化物,嵌入的氧化铝颗粒在粘合剂区域中优先发现,而对于WC-Co硬质合金,氧化铝颗粒更均匀地分布。我们建议一种优先嵌入DC复合材料的粘合剂区域中的氧化铝颗粒的机制,并要求如常规WC-CO相比,这种优先嵌入对这些复合材料的观察到的低磨损系数负责。

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