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Rapid and Facile Synthesis of Monodisperse α-Bi_2O_3 Nanowires by Solution Precipitation Method

机译:通过溶液沉淀法快速且容易合成单分散α-Bi_2O_3纳米线

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Monodisperse α-Bi_2O_3 nanowires with the diameter of 50-100 nm and the length-diameter ratio of 60-100, were synthesized successfully by solution precipitation method, an efficient and convenient route, with the assistance of oleic acid. X-ray diffraction (XRD) and field-emission scanning electron microscope (FE-SEM) were employed to characterize the obtained products. By analyzing the influential factors, it was found that the size and morphology of α-Bi_2O_3 nanowires were affected mainly by temperature, reagent concentration, drip feed speed, and reaction time. It was found that oleic acid played a crucial role in the formation process of nanowires. And the optimum synthesis conditions were identified to prepare the final products to meet the needs of application.
机译:通过溶液沉淀法,在油酸的帮助下成功地合成了直径为50-100nm和60-100的长度直径比为60-100的单向α-Bi_2O_3纳米线。使用X射线衍射(XRD)和现场 - 发射扫描电子显微镜(Fe-SEM)来表征所得产物。通过分析影响因素,发现α-Bi_2O_3纳米线的尺寸和形态主要受温度,试剂浓度,滴注进料速度和反应时间影响。发现油酸在纳米线的形成过程中发挥着至关重要的作用。鉴定了最佳的合成条件以准备最终产品以满足应用需求。

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