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Wet Granulation of Fumed Silica

机译:湿法造粒熏蒸二氧化硅

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Pin mixers are frequently used to convert fine particles into larger ones. Powder, liquid (preferably water), and binder are fed into a pin mixer, which consists of an agitator comprised of pins on a horizontal rotating shaft inside an enclosed chamber. The relative rates of coalescence and attrition and the time inside the pin mixer determine the final particle size distribution. The “green” or wet agglomerates that leave the pin mixer must have sufficient strength to withstand the downstream drying process. The strength of a green pellet highly depends on its saturation state, which is the fraction of the void volume of the agglomerates that contain water. Green agglomerates from a pin mixer are the most durable when at their funicular state of saturation, which exists when water begins to accumulate at the contact points between individual particles. At lower moisture contents, dry particles exist, which can turn into dust. Too high a moisture content will reduce the capillary forces that hold the particles together, and if appreciably high, a paste or slurry may be created. Saturation states are illustrated in Figure 1.
机译:销混合器经常用于将细颗粒转化为更大的颗粒。粉末,液体(优选水)和粘合剂被加入销混合器中,该销混合器由封闭腔室内的水平旋转轴上构成的搅拌器组成。聚结和磨损的相对速率以及销混合器内的时间确定最终的粒度分布。离开销混合器的“绿色”或湿聚集必须具有足够的强度以承受下游干燥过程。绿色颗粒的强度高度取决于其饱和状态,这是含有水的附聚物的空隙体积的一部分。来自销混合器的绿色凝聚是最耐用的,当它们在其磁性饱和状态下,当水开始在各个颗粒之间的接触点处积聚时存在。在较低的水分含量下,存在干燥的颗粒,其可以变成灰尘。太高的水分含量将减少将颗粒固定在一起的毛细管力,并且如果明显高,则可以产生糊状或浆料。饱和状态在图1中示出。

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