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High-Resolution Characterisation of Austenitic Stainless Steel in PWR Environments: Effect of Strain and Surface Finish on Crack Initiation and Propagation

机译:PWR环境中奥氏体不锈钢的高分辨率表征:应变和表面光洁度对裂纹启动和繁殖的影响

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摘要

Initiation and propagation of cracks under simulated primary water conditions and different slow strain rates have been studied for an austenitic 304-type stainless steel. Two surface finishes were used to better understand the conditions that trigger stress corrosion cracking (SCC). The main objective is to identify the mechanism(s) that govern the initiation and propagation of SCC and the influence of microstructure. Crack morphology, stress localisation and local chemical composition were characterized for all samples studied. The characterization methodology includes scanning electron microscopy (SEM), 3D focused ion beam (FIB), Transmission Kikuchi Diffraction (TKD), and analytical scanning transmission electron microscopy (STEM).
机译:已经研究了模拟初级水条件下裂缝的启动和传播,并针对奥氏体304型不锈钢研究了不同的慢率速率。使用两个表面饰面来更好地理解触发应力腐蚀裂纹(SCC)的条件。主要目的是鉴定控制SCC的启动和传播的机制以及微观结构的影响。裂纹形态,应力定位和局部化学成分的特征在于研究的所有样品。表征方法包括扫描电子显微镜(SEM),3D聚焦离子束(FIB),传输Kikuchi衍射(TKD)和分析扫描透射电子显微镜(茎)。

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