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Molybdenum oxide Nanocubes: Synthesis and characterizations

机译:氧化钼纳米孔:合成和表征

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Molybdenum oxide nanoparticles were prepared by Solid state synthesis. The MoO_3 nanoparticles were synthesized by using commercially available ammonium heptamolybdate. The XRD pattern reveals that the synthesized MoO_3 has orthorhombic structure. In addition, lattice parameter values were also calculated using XRD data. The Raman analysis confirm the presence of Mo-O in MoO_3 nanoparticles. DRS-UV analysis shows that MoO_3 has a band gap of 2.89 eV. FE-SEM analysis confirms the material morphology in cubes with nano scale.
机译:通过固态合成制备氧化钼纳米粒子。通过使用市售的氨基钼酸盐合成MOO_3纳米颗粒。 XRD图案显示合成的MOO_3具有正交结构。此外,还使用XRD数据计算格子参数值。拉曼分析证实了MOO_3纳米颗粒中MO-O的存在。 DRS-UV分析表明Moo_3具有2.89eV的带隙。 Fe-SEM分析证实了纳米规模的立方体中的物质形态。

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