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Palm-top size X-ray microanalyzer using a pyroelectric focused electron beam with 100-micro-meter diameter

机译:掌上尺寸的X射线微分析仪采用热电聚焦电子束,具有100微米直径

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We have developed a palm-top size EPMA (electron probe X-ray microanalyzer), operated by 3 V electric battery except for a rotary vacuum pump.The electron beam was generated by a pyroelectric single crystal, LiTaO_3.A needle was used to make a focused electron beam.The smallest beam size was 100 μm on the sample surface.The X-ray spectra were measured through a Kapton window by a Si-PIN detector for a model specimen containing TiO_2 and MnO_2 particles, which was an aerosol model specimen, where TiO_2 and MnO_2 particles of size about 100-200 μm were separated by a few hundreds micrometers.By moving the sample stage manually, the X-ray spectra were measured for 300 s each by 300 μm e-beam, and the measured X-ray intensities were strong enough for identification of the major element in individual 100-200 μm size aerosol particles.
机译:我们开发了一种掌上尺寸的EPMA(电子探针X射线微Zalyzer),除了旋转真空泵之外,通过3V电动电池操作。电子束由热电单晶产生,LiTaO_3.A针用于制造在样品表面上最小的光束尺寸为100μm。通过Si-PIN检测器通过Kapton窗口测量X射线光谱,用于含有TiO_2和MnO_2颗粒的模型样品,这是气溶胶模型样本,其中大小约100-200μm的TiO_2和MnO_2颗粒被几百微米分离。通过手动移动样品级,测量X射线光谱,每个X射线谱分别为300μm射束,测量x - 射线强度足以识别单个100-200μm尺寸气溶胶颗粒中的各个主要元素。

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