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A Fully Automated Multiple Injection On-line SPE-LC-MS/MS Method for Analysis of Trace Level Drug Residues in Water

机译:全自动多次注射在线SPE-LC-MS / MS方法,用于分析水中痕量药物残留物

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摘要

The results of this study show that multi-injection method for on-line SPE LC-MS/MS analysis of trace level water samples does not cause any loss of trapped compounds. Enhanced recoveries were obtained by more consecutive injections of low concentration water samples compared to less number of injections of higher concentration water sample. This preliminary finding suggests that multi-injection method is potentially useful for on-line SPE LC-MS/MS method for analysis of trace level pharmaceutical compounds in water samples as well as other applications.
机译:该研究的结果表明,用于线SPE LC-MS / MS分析的多注射方法对痕量水样的分析不会导致任何捕获的化合物损失。通过更高浓度水样的注射量相比,通过更加连续注射低浓度水样品获得增强的回收率。该初步发现表明,多喷射方法可能对在线SPE LC-MS / MS / MS方法中有用,用于分析水样中的痕量药物化合物以及其他应用。

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