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Fabrication of Lotus--type Porous Alumina with High Compressive Strength Using Unidirectional Solidification

机译:用单向凝固制备莲型多孔氧化铝,具有高抗压强度

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Lotus-type porous alumina was fabricated by unidirectional solidification under hydrogen gas flow (0.1 MPa) and pressurized hydrogen atmosphere using silica and calcia added alumina feed rods. The silica and/or calcia additives in the feed rods strongly affect on the formation of porous structure during the solidification. The porosity increases with increasing silica content. The added calcia in the feed rod is effective on the homogenization of pore distribution. The pores are elongated along the solidification direction. The pores were increased in length when the solidification was performed in pressurized hydrogen atmosphere. A glassy boundary phase which was consisted of silica and calcia components was directly formed in the solidified sample during the solidification. The compressive strength of porous sample with 25.9 percent porosity and non-porous sample prepared in Ar atmosphere were 512 and 1679 MPa, respectively.
机译:通过在氢气流量(0.1MPa)下的单向凝固和使用二氧化硅和氧化钙加入的氧化铝进料棒来制造莲型多孔氧化铝。进料杆中的二氧化硅和/或氧化钙添加剂强烈影响凝固过程中多孔结构的形成。随着二氧化硅含量的增加,孔隙率增加。进料棒中添加的氧化钙对孔分布的均质化有效。孔沿凝固方向伸长。当在加压氢气氛中进行凝固时,孔的长度增加。在凝固过程中直接在固化样品中直接形成由二氧化硅和钙染色组分组成的玻璃状边界相。多孔样品的抗压强度分别具有25.9%的孔隙率和在Ar气氛中制备的无多孔样品为512和1679MPa。

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