首页> 外文会议>International Conference on Fracture >EXPERIMENTAL INVESTIGATION OF STRAIN, DAMAGE AND FAILURE OF HYDRIDED ZIRCONIUM ALLOYS WITH VARIOUS HYDRIDE ORIENTATIONS
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EXPERIMENTAL INVESTIGATION OF STRAIN, DAMAGE AND FAILURE OF HYDRIDED ZIRCONIUM ALLOYS WITH VARIOUS HYDRIDE ORIENTATIONS

机译:各种氢化物取向氢化锆合金菌株,损伤和失效的实验研究

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This experimental investigation is devoted to the hydride embrittlement of fuel cladding tubes and especially to the influence of the orientation of hydrides with respect to the applied stress on strain, damage and failure mechanisms. Ring tensile tests are performed on cladding tube material (unirradiated cold worked stress-relieved Zircaloy-4). The average hydrogen content of the material is about 200ppm, and orientations of hydrides are either "tangential" (hydride platelets parallel to the tensile direction) or "radial" (perpendicular to the tensile direction). Tangential hydrides are usually observed in cladding tubes, in particular because of the texture of the material. However, hydrides can be reoriented after cooling under stress and become radial and then trigger brittle behaviour. In this investigation, we first perform "macroscopic" tensile tests, on smooth rings, which give us the mechanical response of the material as a function of hydride orientation. Then, we perform SEM in-situ tensile tests, on rings with the same geometry, in order to observe damage and failure mechanisms. In both cases, digital image correlation techniques are used to estimate local and global strain levels. For macroscopic tests, airbrush speckle painting is used to mark the samples while 2μm-pitch micro-grids are used for in-situ tests. The "macroscopic" tests underline the strong influence of the hydrides orientation: the specimen with radial hydrides suddenly fails at 1700N, within the elastic domain, whiles the specimen with tangential hydrides reaches 4300N and develops macroscopic shear band. The SEM in-situ tests allow us to improve the understanding of failure mechanisms: with radial hydrides, a crack propagates along a path of aligned hydrides and leads to failure. With tangential hydrides, macroscopic shear bands lead to large plastic strain and final ductile failure; damage can only be observed in the very late stage of deformation.
机译:该实验研究致力于燃料包层管的氢化物脆化,尤其是氢化物的取向相对于施加应力的影响,损伤和破坏机制的影响。环形拉伸试验是在包层材料(未照射的冷加工应力Zircaloy-4)上进行的。材料的平均氢含量约为200ppm,氢化物的取向是“切向”(平行于拉伸方向的氢化物血小板)或“径向”(垂直于拉伸方向)。通常在熔覆管中观察到切向氢化物,特别是因为材料的质地。然而,在胁迫下冷却后可以重新定位氢化物,然后变得径向,然后触发脆性行为。在这次调查中,我们首先在光滑环上进行“宏观”拉伸试验,这使得能够作为氢化物取向的函数的材料的机械响应。然后,我们在具有相同几何形状的环上执行SEM的原位拉伸试验,以观察损坏和故障机制。在这两种情况下,数字图像相关技术用于估计局部和全局应变级别。对于宏观测试,喷枪斑点涂漆用于标记样品,而2μm间距微网用于原位测试。 “宏观”试验强调氢化物取向的强烈影响:具有径向氢化物的样品在1700n中突然在弹性域内失效,与切向氢化物的样品达到4300N并发显影宏观剪切带。 SEM的原位测试允许我们改善对失效机制的理解:通过径向氢化物,裂纹沿着对齐的氢化物的路径传播并导致失效。通过切向氢化物,宏观剪切带导致大的塑性菌株和最终的延展性衰竭;只有在变形的最晚阶段只能观察到损坏。

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