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INDENTATION FRACTURE, ACOUSTIC EMISSION AND MODELLING OF THE MECHANICAL PROPERTIES OF THIN CERAMIC COATINGS

机译:缩进骨折,声学发射和薄陶瓷涂层机械性能的建模

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Fracture is an almost inevitable consequence of highly loaded contacts in ceramic-coated systems. For relatively thick coatings fracture is often similar to that observed in bulk samples of the coating but as the coating thickness is reduced the substrate plays an increasing role in influencing or even controlling fracture behaviour. Both through-thickness and interfacial fracture may be observed depending on the relative toughness of the substrate, coating and interface. Through-thickness fracture is exacerbated by plastic deformation in the substrate and therefore the load support from the substrate is critically important in determining the type and extent of fracture observed. In this paper, nanoindentation testing and post facto atomic force and scanning electron microscopy is used to characterise the types of fracture which occur for hard coatings on softer substrates and multilayer coatings on glass. The effect of fracture on the nanoindentation load-displacement curves and the hardness and Young's Modulus values obtained from them is discussed and a simple model to account for the observed behaviour is introduced. The use of acoustic emission to monitor plasticity and fracture during the indentation cycle is also discussed.
机译:骨折是陶瓷涂层系统中高负荷接触的几乎不可避免的后果。对于相对厚的涂料裂缝通常与涂层的块状样品中观察到的裂缝,而随着涂层厚度降低,基材在影响甚至控制骨折行为方面发挥着越来越大的作用。可以根据基板,涂层和界面的相对韧性来观察到贯穿厚度和界面骨折。通过基板中的塑性变形加剧了贯穿厚度裂缝,因此在确定观察到的裂缝的类型和程度方面,来自基板的负载载体至关重要。在本文中,纳米狭窄测试和后事实上的原子力和扫描电子显微镜用于表征骨折的硬涂层的裂缝类型和玻璃上的多层涂层。讨论了裂缝对纳米狭窄负荷 - 位移曲线的影响以及从它们获得的硬度和杨氏模数值,并介绍了用于观察到的行为的简单模型。还讨论了在压痕周期期间监测可塑性和骨折的声学发射。

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