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Oil Bath for Precision Calibration of Thermometers in the Range 90°C to 200°C

机译:用于90°C至200°C的温度计的精确校准的油浴

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The calibration of thermometers requires a stable environment. In the range 90°C to 200°C normally comparison calibrations are performed in liquid baths with silicone oil as the fluid medium. This range is difficult to cover with sufficient temperature stability using commercially available baths. Therefore a calibration bath was constructed in our laboratory and presented at the 21st Nordic conference on Measurements and Calibration in 1999. The experience from this has led to this further improved version. The principle of the bath is based on a closed end aluminum tube, with an inner open concentric tube placed near the bottom and allowing free circulation of the oil around it. The circulation is achieved by a stirring propeller in the lower end, and the calibration zone is located inside the inner tube. The heating power is supplied by two different heaters, one main heater wrapped on the outside of the outer tube and one placed in the space between the cylinders. The main heater acts as a guard heater and is supplied with constant power to give the outer wall a stable temperature, just below the set point. The second smaller heater performs the regulation with the aid of a commercial controller. The bath is housed in a floor cabinet and has a working space of diameter 100 mm and a depth of 500 mm. Temperature stability and uniformity achieved in the bath is around +-1 mK in the whole range up to 200°C, and this is without the use of any kind of equalising block. This is an improvement from the earlier version in the upper temperature range. For example temperature instability and nonuniformity has decreased from +-3 mK to +-1 mK at 200°C. The performance is now comparable with the best water baths used at lower temperatures. Data and diagrams are presented in this paper.
机译:温度计的校准需要稳定的环境。在90°C至200°C的范围内,通常在液体浴中使用硅油作为流体介质进行比较校准。该范围难以使用市售的浴剂具有足够的温度稳定性。因此,在我们的实验室中构建了校准浴,并在1999年在21世纪的测量和校准会议上提出。这一切的经验导致了这一进一步改进的版本。浴的原理基于封闭端铝管,内部开放的同心管放置在底部附近,并允许其周围的油循环。通过下端的搅拌螺旋桨实现循环,并且校准区位于内管内。加热功率由两个不同的加热器提供,一个主加热器包裹在外管的外侧,一个主加热器缠绕在气缸之间的空间中。主加热器用作护罩加热器,并提供恒定的功率,以使外壁具有稳定的温度,在设定点以下。第二个较小加热器借助于商业控制器执行调节。浴缸容纳在地板柜中,并且具有100mm直径的工作空间,深度为500毫米。在浴缸中实现的温度稳定性和均匀性在整个范围内达到约200°C,而不是使用任何类型的均衡块。这是从上温度范围内的早期版本的改进。例如,温度不稳定性和不均匀性在200℃下从+ -3 mk到+ -1 mk降低。该性能现在与在较低温度下使用的最佳水浴相当。本文提出了数据和图表。

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