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Preparation of Nano-sized Strontium Containing Tricalcium Phosphate Particles

机译:含有磷酸三钙颗粒的纳米锶的制备

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In this work, nano-sized strontium containing tricalcium phosphate (SrTCP) particles with different strontium content were prepared using co-precipitation method in an ice-water bath and then 800°C calcination. The AAS results show that the relative Sr/(Sr+Ca) ratios are consistent with the amount of strontium added in the initial solution but larger than the designed molar percentage. The TEM micrographs demonstrate the size of the SrTCP particles is in the region of 150-400 nm while the pure TCP particle is about 500nm. The SEM photographs show the morphology of the particles before and after incorporation of strontium and it is obvious that the particle size of SrTCP decrease with the increasing of strontium content.
机译:在这项工作中,使用共沉淀法在冰水浴中使用共沉淀法制备含有不同锶含量的含有不同锶含量的纳米尺寸锶(SRTCP)颗粒,然后在800℃煅烧中制备。 AAS结果表明,相对SR /(SR + Ca)比率与初始溶液中加入的锶量一致,但大于设计的摩尔百分比。 TEM显微照片显示SRTCP颗粒的尺寸在150-400nm的区域中,而纯TCP颗粒约为500nm。 SEM照片显示锶前后颗粒的形态,并且显然SRTCP的粒径随着锶含量的增加而降低。

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