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Surface potential measurement of electrically poled hap ceramics

机译:电极高清陶瓷的表面电位测量

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The surface morphology and surface potential of the hydroxyapatite (HAp) ceramics with and without electrically poling were first investigated by tapping mode atomic force microscopy (TMAFM) combined with surface potential microscopy (SPoM). The HAp ceramic specimens were prepared by sintering the compact bodies of wet-chemically synthesized powders at 1250 deg C for 2 h under H_2O flow. The specimen was partially polarized in a dc field of 1000 V cm~(-1) for 1 h in air at 300 deg C. The surface potential distribution on the HAp specimen were significantly different between unpolarized surface and polarized one; the surface potential of polarized HAp region was higher than that of unpolarized one. The acceleration and deceleration of in vitro bonelike crystal growth on HAp ceramics soaking in a simulated body fluid solution could be related to the surface potential change caused by the electrically poling.
机译:首先通过挖掘模式原子力显微镜(TMAFM)与表面电位显微镜(SPOM)结合来研究羟基磷灰石(HAP)陶瓷的表面形态和表面电位。通过在1250℃下在H_2O流下烧结湿化化学合成粉末的紧凑型体来制备HAP陶瓷样品。在300℃的空气中,将样品在1000Vcm〜(-1)的DC场中部分偏振,在300℃下在空气中。HAP样本的表面电位分布在非偏振表面和偏振之间的显着差异;偏振HAP区域的表面电位高于非偏振的表面电位。在模拟体液溶液中浸泡在模拟体液溶液中的体外合成晶体生长的加速和减速可能与由电极引起的表面电位变化有关。

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