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Vacuum Infusion Process Development for Conformal Ablative Thermal Protection System Materials

机译:保形烧蚀热保护系统材料的真空灌注工艺开发

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Conformal ablators are low density composite materials comprised of a flexible fibrous substrate and polymer matrix. These materials are fabricated to near net shape by placing the substrate in a rigid, matched mold and infusing with liquid resin in an open, vacuum-assisted immersion process. This process, originally developed for older rigid substrate ablators such as PICA, wastes a substantial amount of resin. In this work, a vacuum infusion process - a type of liquid composite molding where resin is directly injected into a closed mold under vacuum — is advanced for conformal ablators. The process reduces waste over the state-of-the-art technique and may eliminate the need for an atmosphere-controlled oven. Small, flat samples of Conformal Phenolic Impregnated Carbon Ablator are infused using the new approach and subjected to a range of curing configurations and conditions. Resulting materials are inspected for quality and compared to material produced using the standard process. Density, resin mass fraction and char yield are measured. Lessons learned inform subsequent plans for process scale up.
机译:保形的消融器是低密度的复合材料,由柔性纤维基材和聚合物基质组成。通过将基板放在刚性,匹配的模具中,并在开放的真空辅助浸入过程中注入液态树脂,可以将这些材料制成接近最终的形状。此工艺最初是为较旧的刚性基材烧蚀器(如PICA)开发的,浪费了大量的树脂。在这项工作中,采用了真空灌注工艺(一种液态复合成型工艺,其中将树脂在真空下直接注入密闭模具中)用于共形烧蚀器。与现有技术相比,该工艺减少了浪费,并且可以消除对可控气氛烤箱的需要。使用新方法注入小的,扁平的共形酚醛浸渍碳消融剂样品,并经受一系列固化配置和条件。检查所得材料的质量,并将其与使用标准工艺生产的材料进行比较。测量密度,树脂质量分数和炭收率。所汲取的经验教训可为后续流程扩展计划提供参考。

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