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FABRICATION OF 2.5D ROCK-BASED MICROMODELS WITH HIGH RESOLUTION FEATURES

机译:具有高分辨率的2.5D岩石微模型的制作

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Fabrication of 2.5D rock-based micromodels with high resolution features is presented using SU-8 multi-layer lithography and nickel electroforming for nickel molds. Processes associated with SU-8 were carefully optimized by the use of the vacuum contact, the use of UV filter, and controls of UV exposure doses and baking times. The use of SU-8 MicroSpray enabled the easy fabrication of multi-layers of SU-8, while exhibiting some total thickness variations. The thirteen layered SU-8 samples showed reliable patterning results for features at 10 and 25 μm resolutions, and minor pattern distortions of features at the 5 μm resolution. Flycutting method employed in multi-layer lithography of SU-8 yielded accurate total thickness control within ±1.5 μm and excellent pattern formation for all of 5, 10, and 25 μm features. Electroforming of nickel was optimized with electroplating bath composition and electroplating parameters such as current density to realize the high resolution nickel mold. The fabricated nickel molds from flycutting based SU-8 samples revealed the feasibility of manufacturing the minimum features down to 5 μm for thirteen layers without any pattern distortions. The replication-based micromolding method will allow for fabrication of micromodels in a variety of materials such as polymers and ceramics. The high resolution, 2.5D micromodels will be used for investigation of pore-scale fluid transport, which will aid in understanding the complicated fluidic phenomena occurring in the 3D reservoir rock.
机译:使用SU-8多层光刻技术和用于镍模的镍电铸技术,展示了具有高分辨率特征的2.5D岩石微模型的制造。通过使用真空接触,使用紫外线过滤器以及控制紫外线照射剂量和烘烤时间,精心优化了与SU-8相关的工艺。 SU-8 MicroSpray的使用使SU-8的多层结构易于制造,同时总厚度有所变化。十三个SU-8样品在分辨率为10和25μm的情况下显示出可靠的构图结果,在分辨率为5μm的情况下显示出较小的特征图形失真。 SU-8的多层光刻中使用的快速切割方法可将精确的总厚度控制在±1.5μm之内,并且对于5、10和25μm的所有特征均具有出色的图案形成能力。利用电镀液成分和电流密度等电镀参数对镍的电铸工艺进行优化,以实现高分辨率的镍铸模。由基于飞切的SU-8样品制成的镍模显示出了制造13层最小5μm最小特征而没有任何图案变形的可行性。基于复制的微成型方法将允许在多种材料(例如聚合物和陶瓷)中制造微模型。高分辨率的2.5D微观模型将用于研究孔隙尺度的流体传输,这将有助于理解3D油藏岩石中发生的复杂流体现象。

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