Synthesis of Bis(triiodopyrazole)s as Intermediates for HEMs

机译：双（三碘吡唑）s作为HEMs中间体的合成

获取原文

页面导航

摘要
著录项
相似文献
相关主题

摘要

Bis(3,4,5-triiodopyrazolyl)methane (1) and bis(3,4,5-triiodopyrazolyl)ethane (2), which could be effective intermediates for the high energetic materials (HEMs), were synthesized in 56％ and 55％ yields, respectively, from 3,4,5-triiodopyrazole.The synthesized bis(triiodopyrazole)s were fully characterized by differential-scanning calorimeter, 1H, 13C-NMR analyses and high resolution mass spectroscopy.

机译：双（3,4,5-三碘并吡唑基）甲烷（1）和双（3,4,5-三碘并吡唑基）乙烷（2）可能是高能材料（HEM）的有效中间体，合成率为56％， 3,4,5-三碘吡唑的产率分别为55％。通过差示扫描量热仪，1 H，13 C-NMR分析和高分辨率质谱对合成的双（三碘吡唑）进行了充分表征。

著录项

来源
《Beijing Institute of Technology;China Ordnance Society;International autumn seminar on propellants, explosives and pyrotechnics;Hubei Institute of Aerospace Chemotechnology》|2015年|8-10|共3页
会议地点
作者
Byeongil LEE; Moonyong SHIN; Namtae KIM; Junghwan OH; Jin Seuk KIM; Young Gyu KIM;
展开▼
作者单位

展开▼
会议组织
原文格式 PDF
正文语种
中图分类爆炸物工业、火柴工业;
关键词
explosives; iodopyrazole; bisazole;

机译：炸药;碘吡唑;双唑;

相似文献

外文文献
中文文献
专利

1. SYNTHESIS OF 1-[3,5-BIS-(2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSYL)-,2,4,6-TRIHYDROX YPHENYL]ETHANONE - AN INTERMEDIATE OF POTENTIAL USEFULNESS FOR SYNTHESIS OF BIS-C-GLUCOSYL FLAVONOIDS [J] . Kumazawa T., Matsuba S., Sato S., Carbohydrate research . 1997,第4期

机译：1- [3,5-BIS-（2,3,4,6-四-O-乙酰基-贝塔-D-葡糖基糖基）-，2,4,6-三羟基苯乙炔]乙酮的合成-潜在的高可用性用于合成BIS-C-葡糖基黄酮
2. SYNTHESIS AND CHARACTERIZATION OF A BIS(MU-BETA-DIKETONATO)BIS((1,2,5,6-ETA)-1,5-DIMETHYL-1,5-CYCLAOCTADIENE)D ISILVER COMPLEX - AN INTERMEDIATE IN THE SYNTHESIS OF AN ISOMERICALLY PURE (BETA-DIKETONATO)((1,2,5,6-ETA)-1,5-DIMETHYL-1,5-CYCLOOCTADIENE) [J] . Doppelt P., Ricard L., Baum TH. Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 1996,第5期

机译：BIS（MU-BETA-DIKETONATO）BIS（（1,2,5,6-ETA）-1,5-DIMETHYL-1,5-CYCLCTCTADIENE）D Silver Complex-中间体的合成与表征异构纯（BETA-DIKETONATO）（（（1,2,5,6-ETA）-1,5-DIMETHYL-1,5-CYCLOCCTADIENE）
3. SYNTHESIS AND CHARACTERIZATION OF A BIS(MU-BETA-DIKETONATO)BIS((1,2,5,6-ETA)-1,5-DIMETHYL-1,5-CYCLAOCTADIENE)D ISILVER COMPLEX - AN INTERMEDIATE IN THE SYNTHESIS OF AN ISOMERICALLY PURE (BETA-DIKETONATO)((1,2,5,6-ETA)-1,5-DIMETHYL-1,5-CYCLOOCTADIENE) [J] . Doppelt P., Ricard L., Baum TH. Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 1996,第5期

机译：BIS（MU-BETA-DIKETONATO）BIS（（1,2,5,6-ETA）-1,5-DIMETHYL-1,5-CYCLCTCTADIENE）D Silver Complex-中间体的合成与表征异构纯（BETA-DIKETONATO）（（（1,2,5,6-ETA）-1,5-DIMETHYL-1,5-CYCLOCCTADIENE）
4. Synthesis of Bis(triiodopyrazole)s as Intermediates for HEMs [C] . Byeongil LEE, Moonyong SHIN, Namtae KIM, International autumn seminar on propellants, explosives and pyrotechnics . 2015

机译：双（三碘葡萄唑）作为下摆中间体的合成
5. Part I. Synthesis of N-substituted 2,5-bis-[4-guanidinophenyl]thiophenes as potential antileishmanial compunds. Part II. Synthesis of novel potential prodrugs of bis-guanidino and bis-amidino molecules. [D] . Gonzalez-Roman, Jose Luis. 2002

机译：第一部分：N-取代的2,5-双-[4-胍基苯基]噻吩的合成作为潜在的抗衰老化合物。第二部分双胍基和双-基分子的新型潜在前药的合成。
6. Data for the synthesis and characterisation of 26-di(bromomethyl)-35-bis(alkoxycarbonyl)-4-aryl-14-dihydropyridines as important intermediates for synthesis of amphiphilic 14-dihydropyridines [O] . Martins Rucins, Klavs Pajuste, Arkadij Sobolev, 2020

机译：26-二（溴甲基）-35-双（烷氧基羰基）-4-芳基-14-二氢吡啶的合成和表征数据是合成两亲性14-二氢吡啶的重要中间体
7. Control of Photosynthetic Sucrose Synthesis by Fructose 2,6-Bisphosphate 1: VI. Regulation of the Cytosolic Fructose 1,6-Bisphosphatase in Spinach Leaves by an Interaction between Metabolic Intermediates and Fructose 2,6-Bisphosphate [O] . Stitt, Mark, Heldt, Hans W. 1985

机译：果糖2，6-二磷酸1：VI控制光合蔗糖的合成。代谢中间体和果糖2，6-二磷酸之间的相互作用调节菠菜叶中的胞质果糖1，6-Bisphosphatase。

Synthesis of Bis(triiodopyrazole)s as Intermediates for HEMs

摘要

著录项

相似文献

相关主题

期刊订阅