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Interfacial Behavior of Micro-cellular Structural Al_(90)Mn_9Ce_1/TiO_2 Composite Prepared by Spark Plasma Sintering

机译:放电等离子烧结制备微孔结构Al_(90)Mn_9Ce_1 / TiO_2复合材料的界面行为

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With micron Al_(90)Mn_9Ce_1/TiO_2 alloy powder clad by TiO_2 nano-powder, a dense closed micro-cellular ceramics structure was fabricated. The alloy composite was filled inside by spark plasma sintering at temperature 793 K, and with the composite density of 98.2%. Micro-temperature area of Al_(90)Mn_9Ce_1/TiO_2 matrix was simulated through ANSYS, and the macro lower temperature sintering mechanism was analyzed. The microstructure of the interface was investigated via scanning electron microscope, and the composition distribution of the interface was investigated via energy dispersive spectrometry. The formation and evolution of the interfaces were analyzed from plastic deformation, the interface creep, interfacial diffusion and other aspects. It was found that the application of DC pulse current has important effect on interfacial behavior and the performance of composite.
机译:以TiO_2纳米粉为包覆的微米Al_(90)Mn_9Ce_1 / TiO_2合金粉末,制备了致密的密闭微孔陶瓷结构。通过在793 K的温度下通过火花等离子体烧结将合金复合材料填充到内部,并且复合材料密度为98.2%。通过ANSYS模拟了Al_(90)Mn_9Ce_1 / TiO_2基体的微温区,并分析了宏观低温烧结机理。通过扫描电子显微镜研究界面的微观结构,并通过能量色散光谱法研究界面的组成分布。从塑性变形,界面蠕变,界面扩散等方面分析了界面的形成和演化。发现直流脉冲电流的施加对界面行为和复合材料的性能具有重要影响。

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