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Thermal evaporation synthesis and properties of ZnO nano/microstructures using Sn reducing agents

机译:锡还原剂对ZnO纳米/微结构的热蒸发合成及性能

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ZnO nano/microstructures have been successfully synthesized via the thermal evaporation mothed using Sn powders as the reducing agents. The as-synthesized products have been systematically studied by X-ray powder diffraction (XRD), Raman spectroscopy (RS), scanning electron microscope (SEM), electron energy-dispersive X-ray (EDX) and ultraviolet-visible spectrum (UV-vis). The results indicate that pure ZnO and Zn2SnO4-doped ZnO were collected at the growth temperatures of 600 °C and 750 °C, respectively. Furthermore, the band gap energy of the as-synthesized product is estimated to be smaller than the reported value for ZnO. The Zn2SnO4 phase in the ZnO nano/microstructures plays an important role in the optical property.
机译:通过使用锡粉作为还原剂的热蒸发法成功地合成了ZnO纳米/微结构。通过X射线粉末衍射(XRD),拉曼光谱(RS),扫描电子显微镜(SEM),电子能量分散X射线(EDX)和紫外可见光谱(UV-可见)。结果表明,分别在600°C和750°C的生长温度下收集到纯ZnO和Zn2SnO4掺杂的ZnO。此外,估计合成后产物的带隙能小于ZnO的报告值。 ZnO纳米/微结构中的Zn2SnO4相在光学性质中起重要作用。

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