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The study on preparation of ZnO nanowire in AAO by electrodeposition method

机译:电沉积法制备AAO中ZnO纳米线的研究

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Ordered zinc oxide (ZnO) nanowire arrays embedded in anodic aluminum oxide (AAO) template were fabricated by electrodepositing zinc (Zn) and then oxidizing the deposited Zinc. The microstructures and compositions of Zn/AAO, ZnO/AAO assemblies were characterized by field emission scanning electron microscopy (FE-SEM) and X-ray diffraction (XRD). The results indicate that the Zn nanowire arrays are uniformly assembled into the nanochannels of AAO with the high filling ratio. Through a thermal treatment in oxygen atmosphere at 700°C for 36 h, the deposited Zinc oxidized completely. Photoluminescence (PL) measurement of the ZnO/AAO assembly exhibits a strong 496 nm emission band which is contributed by the various defects of ZnO.
机译:通过电沉积锌(Zn),然后氧化沉积的锌来制造嵌入阳极氧化铝(AAO)模板中的有序氧化锌(ZnO)纳米线阵列。通过场发射扫描电子显微镜(FE-SEM)和X射线衍射(XRD)对Zn / AAO,ZnO / AAO组件的微观结构和组成进行了表征。结果表明,Zn纳米线阵列被均匀地组装到具有高填充率的AAO的纳米通道中。通过在氧气气氛中于700°C进行36小时的热处理,沉积的锌被完全氧化。 ZnO / AAO组件的光致发光(PL)测量显示出很强的496 nm发射带,这是由ZnO的各种缺陷引起的。

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