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Preparation and magnetic property of multi-walled carbon nanotube/α-Fe2O3 composites

机译:多壁碳纳米管/α-Fe2O3复合材料的制备及磁性

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In order to attain new functional nanomaterials with good magnetic property,multi-walled carbon nanotubes/hematite (MWNTs/α-Fe2O3) composites were synthesized using the co-deposition method.MWNTs/α-Fe2O3 composites were characterized by X-ray diffractometry (XRD),scanning electron microscopy (SEM),transmission electron microscopy(TEM),Raman spectroscopy and vibrating sample magnetometry (VSM).The experimental results show that the structure and magnetic properties of the MWNTs/α-Fe2O3 composites are related to the heat treatment temperature.MWNTs are modified by α-Fe2O3 nano-particles and α-Fe2O3 nanorods with a diameter of 10-50 nm after being treated at 450 °C.When the heat treatment temperature exceeds 600 °C,MWNTs are only modified by Fe3O4 particles.Furthermore,the MWNTs composites treated at 450 °C and 600 °C have good magnetic behaviour.
机译:为了获得具有良好磁性的新型功能纳米材料,采用共沉积法合成了多壁碳纳米管/赤铁矿(MWNTs /α-Fe2O3)复合材料,并利用X射线衍射法对MWNTs /α-Fe2O3复合材料进行了表征。 XRD),扫描电子显微镜(SEM),透射电子显微镜(TEM),拉曼光谱和振动样品磁法(VSM)。实验结果表明MWNTs /α-Fe2O3复合材料的结构和磁性能与热有关在450°C的温度下进行处理后,用直径为10-50 nm的α-Fe2O3纳米粒子和α-Fe2O3纳米棒对MWNTs进行改性。当热处理温度超过600°C时,仅用Fe3O4对MWNTs进行改性。此外,在450°C和600°C下处理的MWNTs复合材料具有良好的磁性能。

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