Benzene-thermal Synthesis of Environmental Catalytic Material of Iron Nitride Nanoparticle

摘要

Environmental catalytic material of iron nitride nanoparticle was synthesized by Benzene - thermal method. In high-pressure reaction kettle, anhydrous FeCl3 and Li3N were reacted in benzene with nitrogen-flow at 450～500°C and stirred for more than 30 h. XRD showed that Fe4N was the main product and the average crystalline size was about 10nm. The above reaction conditions were easy to control.